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Elaboration and characterization of polyaniline films electrodeposited on tin oxides

Identifieur interne : 003058 ( Main/Repository ); précédent : 003057; suivant : 003059

Elaboration and characterization of polyaniline films electrodeposited on tin oxides

Auteurs : RBID : Pascal:11-0478372

Descripteurs français

Pascal (Inist)
- Aniline polymère, Polymère conducteur, Couche mince, Préparation, Polymérisation électrolytique, Méthode potentiostatique, Méthode potentiodynamique, Couche ITO, Epaisseur couche, Morphologie, Topographie surface, Microrugosité, Etude expérimentale, Couche FTO.

English descriptors

KwdEn :
- Aniline polymer, Conducting polymers, Electrochemical polymerization, Experimental study, ITO layers, Layer thickness, Microroughness, Morphology, Potentiodynamic method, Potentiostatic method, Preparation, Surface topography, Thin film.

Abstract

This paper presents the electrochemical synthesis of polyaniline films on fluorine tin oxide (FTO) and indium tin oxide (ITO) in acidic medium by both potentiodynamic and potentiostatic methods. The use of potentiodynamic deposition showed that conductive polyaniline films were synthesized by the same process than on noble metals and allowed the determination of the electrodeposition potential used for further potentiostatic electrodepositions. The electropolymerization was then performed by chronoamperometry and appeared easier on ITO than on FTO. The electrodeposited polyaniline films were extensively characterized in terms of chemical nature, electrochemical growth, thickness, roughness and morphology. The chemical nature of the films was identified through infrared spectroscopy and X-ray diffraction analyses. The roughness and the morphology of the polymer coatings, determined by profilometry, scanning electron microscopy and atomic force microscopy, were correlated to the calculated thickness of each polyaniline film and to the nature of the substrate.

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Le document en format XML

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<term>Layer thickness</term>
<term>Microroughness</term>
<term>Morphology</term>
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<term>Potentiostatic method</term>
<term>Preparation</term>
<term>Surface topography</term>
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<front><div type="abstract" xml:lang="en">This paper presents the electrochemical synthesis of polyaniline films on fluorine tin oxide (FTO) and indium tin oxide (ITO) in acidic medium by both potentiodynamic and potentiostatic methods. The use of potentiodynamic deposition showed that conductive polyaniline films were synthesized by the same process than on noble metals and allowed the determination of the electrodeposition potential used for further potentiostatic electrodepositions. The electropolymerization was then performed by chronoamperometry and appeared easier on ITO than on FTO. The electrodeposited polyaniline films were extensively characterized in terms of chemical nature, electrochemical growth, thickness, roughness and morphology. The chemical nature of the films was identified through infrared spectroscopy and X-ray diffraction analyses. The roughness and the morphology of the polymer coatings, determined by profilometry, scanning electron microscopy and atomic force microscopy, were correlated to the calculated thickness of each polyaniline film and to the nature of the substrate.</div>
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<fC01 i1="01" l="ENG"><s0>This paper presents the electrochemical synthesis of polyaniline films on fluorine tin oxide (FTO) and indium tin oxide (ITO) in acidic medium by both potentiodynamic and potentiostatic methods. The use of potentiodynamic deposition showed that conductive polyaniline films were synthesized by the same process than on noble metals and allowed the determination of the electrodeposition potential used for further potentiostatic electrodepositions. The electropolymerization was then performed by chronoamperometry and appeared easier on ITO than on FTO. The electrodeposited polyaniline films were extensively characterized in terms of chemical nature, electrochemical growth, thickness, roughness and morphology. The chemical nature of the films was identified through infrared spectroscopy and X-ray diffraction analyses. The roughness and the morphology of the polymer coatings, determined by profilometry, scanning electron microscopy and atomic force microscopy, were correlated to the calculated thickness of each polyaniline film and to the nature of the substrate.</s0>
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Elaboration and characterization of polyaniline films electrodeposited on tin oxides

Elaboration and characterization of polyaniline films electrodeposited on tin oxides

Descripteurs français

English descriptors

Abstract

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Links to Exploration step

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